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Epoxy composite reinforced with nano and micro SiC particles: curing kinetics and mechanical properties

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Date
01/05/2012
Author
Abenojar Buendía, Juana
Martínez Casanova, Miguel Ángel
Pantoja Ruiz, Mariola
Velasco López, Francisco Javier
del Real Romero, Juan Carlos
Estado
info:eu-repo/semantics/publishedVersion
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Abstract
 
 
Epoxy-based composite materials reinforced with hard particles can be used as anti-wear coatings. In this study, a commercial bicomponent resin was used, with 6 and 12% SiC particles in two different particle sizes (nano and 10 µm). The epoxy curing process was studied by Fourier transform infrared spectroscopy (FTIR), differential scanning calorimetry (DSC) and confocal microscopy. Dynamic mechanical thermal analysis (DMTA) tests evaluated the influence of particle additions on the glass transition temperature (T g ). In addition, mechanical properties (hardness and bending strength) and wear resistance were evaluated. The addition of nanometric particles reduced the reaction order. A higher amount of particles decreased T g due to the lower number of crosslinking points. The agglomeration of nano particles led to non-uniform mechanical properties. 6% nano particle addition dramatically improved wear resistance and decreased the friction coefficient.
 
URI
10.1080/00218464.2012.660396
Epoxy composite reinforced with nano and micro SiC particles: curing kinetics and mechanical properties
Tipo de Actividad
Artículos en revistas
ISSN
0021-8464
Materias/ categorías / ODS
Instituto de Investigación Tecnológica (IIT)
Palabras Clave

Cure behavior, mechanical properties, silicon carbide, thermosetting resin.
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